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The calibration solutions were obtained by diluting the stock solutions into the different concentrations 1 µg/mL, 10 µg/mL, 25 µg/mL, 50 µg/mL, 75 µg/mL, and 100 µg/mL with hexane as solvent and the internal standard at 10 µg/mL After vortexing for 10 s, 150 µL was transferred into a 10 mL headspace vial.
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